Table 3: Results of analysis for triamcinolone acetonide (TAM) and benzyl alcohol (BZA) in pure form using the proposed method.
|
|
|
TAM |
|
|
|
BZA |
|
|
|
|
Taken µg/mL |
Found µg/mL |
Recovery % |
Taken µg /mL |
|
Found µg /mL |
Recovery % |
|
|
|
1 |
0.99 |
99.09 |
2 |
|
1.99 |
99.73 |
|
|
|
5 |
|
4.98 |
99.53 |
4 |
|
4.03 |
100.63 |
|
|
10 |
|
10.05 |
100.53 |
6 |
|
6.01 |
100.08 |
|
|
20 |
|
19.98 |
99.91 |
8 |
|
7.94 |
99.19 |
|
|
50 |
|
49.84 |
99.67 |
10 |
|
10.04 |
100.40 |
|
Mean |
|
|
|
99.75 |
|
|
|
100.01 |
|
±SD |
|
|
|
0.53 |
|
|
|
0.02 |
|
±RSD |
|
|
|
0.53 |
|
|
|
0.02 |
|
±SE |
|
|
|
0.24 |
|
|
|
0.019 |
|
Variance |
|
|
|
0.28 |
|
|
|
0.32 |
|
LOD (µg/mL) |
|
|
|
0.19 |
|
|
|
0.15 |
|
LOQ (µg/mL) |
|
|
|
0.62 |
|
|
|
0.46 |