Table 1: Adhesives included in the evaluation with their pH, composition, the percentage in weight of each component and lot number.

Adhesive

Composition

% in Weight

Lot No.

Adper Prompt L- Pop

Bisphenol A diglycidyl ether dimethacrylate (BISGMA)

40-50

419614

pH= 0.8-1

Triethylene glycol methacrylate

40-50

 

 

Tetrabutylammonium tetrafluoroborate

1-10

 

 

Silane-treated silica

1-7

 

 

 

 

 

 

PART A

 

 

 

2-Propenoic acid, 2-Methylropenoic Acid, 2-Methyl, Phosphinicobis (Oxy-2,1-Ethandiyl) Ester 

40

 

 

Mono HEMA Phosphate 

15 - 30

 

 

Methacrylated Pyrophosphates

15 - 30

 

 

Tris 2-(Methacryloyloxy) Ethyl Phosphate

1 - 10

 

 

Ethylene Dimethacrylate 

< 2

 

 

Phosphoric Acid

< 2

 

 

Bis (2,6-Dichlorobenzoyl) Butylphenyl Phosphine Oxide

< 0.2

 

 

2-Hydroxyethyl Methacrylate

< 0.2

 

 

4-Methoxyphenol

< 0.2

 

 

Hydroquinone

< 0.1

 

 

Bisphenol A Diglycidyl Ether Dimethacrylate (BISGMA)

10-15

 

 

DL-Camphorquinone

1-1.5

 

 

Ethyl 4-Dimethylaminobenzoate

<2

 

 

 

 

 

 

PART B

 

 

 

Water

70 - 80

 

 

2-Hydroxyethyl Methacrylate

20 - 30

 

 

2-Propenoic Acid, Polymer with Methylenebutanedioic acid

< 2

 

 

 

 

 

Futurabond NR

PRIMER

 

 

pH= 1.4

Acidic adhesive monomer

50-100

1034373

 

BIS-GMA

5-10

 

 

2-Hydroxyethyl methacrylate

5-10

 

 

 

 

 

 

BONDING

 

 

 

ethanol

50-100

 

 

initiator

2,5-5

 

 

 

 

 

Clearfil SE Bond

PRIMER

 

 

pH= 2

Bisphenol A diglycidyl methacrylate

25-45

00990A

 

2-hydroxyethyl methacrylate

20-40

 

 

 

 

 

 

BONDING

 

 

 

2-hydroxyethyl methacrylate

10-30

01557A

 

Other ingredients:

 

 

 

10-Methacryloyloxydecyl dihydrogen phosphate

 

 

 

Hydrophilic aliphatic dimethacrylate

 

 

 

DL-Camphorquinone

 

 

 

Water

 

 

 

Accelerators

 

 

 

Dyes

 

 

 

Others

 

 

 

 

 

 

AdheSE One F

Bis-methacrylamide dihydrogen phosphate

5-25

NL9016

pH= 1.5

Isopropanol

5-15

 

 

Potassium fluoride

< 1

 

 

Acrylamidosulfonic acid

1-10

 

 

Acrylamido amino acid

5-20

 

 

Water

 

 

 

Alcohol