Table 1: Adhesives included in the evaluation with their pH, composition, the percentage in weight of each component and lot number.
Adhesive |
Composition |
% in Weight |
Lot No. |
Adper Prompt L- Pop |
Bisphenol A diglycidyl ether dimethacrylate (BISGMA) |
40-50 |
419614 |
pH= 0.8-1 |
Triethylene glycol methacrylate |
40-50 |
|
|
Tetrabutylammonium tetrafluoroborate |
1-10 |
|
|
Silane-treated silica |
1-7 |
|
|
|
|
|
|
PART A |
|
|
|
2-Propenoic acid, 2-Methylropenoic Acid, 2-Methyl, Phosphinicobis (Oxy-2,1-Ethandiyl) Ester |
40 |
|
|
Mono HEMA Phosphate |
15 - 30 |
|
|
Methacrylated Pyrophosphates |
15 - 30 |
|
|
Tris 2-(Methacryloyloxy) Ethyl Phosphate |
1 - 10 |
|
|
Ethylene Dimethacrylate |
< 2 |
|
|
Phosphoric Acid |
< 2 |
|
|
Bis (2,6-Dichlorobenzoyl) Butylphenyl Phosphine Oxide |
< 0.2 |
|
|
2-Hydroxyethyl Methacrylate |
< 0.2 |
|
|
4-Methoxyphenol |
< 0.2 |
|
|
Hydroquinone |
< 0.1 |
|
|
Bisphenol A Diglycidyl Ether Dimethacrylate (BISGMA) |
10-15 |
|
|
DL-Camphorquinone |
1-1.5 |
|
|
Ethyl 4-Dimethylaminobenzoate |
<2 |
|
|
|
|
|
|
PART B |
|
|
|
Water |
70 - 80 |
|
|
2-Hydroxyethyl Methacrylate |
20 - 30 |
|
|
2-Propenoic Acid, Polymer with Methylenebutanedioic acid |
< 2 |
|
|
|
|
|
Futurabond NR |
PRIMER |
|
|
pH= 1.4 |
Acidic adhesive monomer |
50-100 |
1034373 |
|
BIS-GMA |
5-10 |
|
|
2-Hydroxyethyl methacrylate |
5-10 |
|
|
|
|
|
|
BONDING |
|
|
|
ethanol |
50-100 |
|
|
initiator |
2,5-5 |
|
|
|
|
|
Clearfil SE Bond |
PRIMER |
|
|
pH= 2 |
Bisphenol A diglycidyl methacrylate |
25-45 |
00990A |
|
2-hydroxyethyl methacrylate |
20-40 |
|
|
|
|
|
|
BONDING |
|
|
|
2-hydroxyethyl methacrylate |
10-30 |
01557A |
|
Other ingredients: |
|
|
|
10-Methacryloyloxydecyl dihydrogen phosphate |
|
|
|
Hydrophilic aliphatic dimethacrylate |
|
|
|
DL-Camphorquinone |
|
|
|
Water |
|
|
|
Accelerators |
|
|
|
Dyes |
|
|
|
Others |
|
|
|
|
|
|
AdheSE One F |
Bis-methacrylamide dihydrogen phosphate |
5-25 |
NL9016 |
pH= 1.5 |
Isopropanol |
5-15 |
|
|
Potassium fluoride |
< 1 |
|
|
Acrylamidosulfonic acid |
1-10 |
|
|
Acrylamido amino acid |
5-20 |
|
|
Water |
|
|
|
Alcohol |
|
|